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State primary standard machine on Vickers and Knoop hardness scales GET 31-2024

https://doi.org/10.32446/0368-1025it.2024-12-7-13

Abstract

The results of research aimed at ensuring the uniformity of hardness measurements according to the Vickers and Knoop scales, reproduction of Vickers hardness numbers HV in the range 2000–5000 and Knoop hardness numbers HK in the range 17–2500. The research is due, firstly, to the fact that the hardness of ceramics used in industry and medicine is more than 2000 HV, and hardness measurements on the Vickers scales of products made of these ceramics were not traced to the State primary special standard for metal hardness on the Vickers GET 31-2010 scales. Secondly, the Vickers tip print has a square shape, therefore, when measuring hardness on a limited area of the surface, for example near a weld, one of the corners of the print goes beyond the boundaries of the measured zone, which leads to an incorrect assessment of the hardness of the studied surface area. The Knoop method, implemented using a tip, the base of which is made in the form of a diamond with one short side, solves the problem of correct hardness testing on a limited area of the surface. A reference installation has been investigated and included in the State primary hardness standard according to the Vickers and Knoop scales GET 31-2024, which allows reproducing the Vickers hardness numbers HV in the range 2000–5000 and the Knoop hardness numbers. Thus, the traceability of measurement results obtained using hardness testers to GET 31-2024 is ensured. The metrological characteristics of GET 31-2024 have been studied. The use of hardness testers traceable to GET 31-2024 makes it possible to accurately assess the mechanical properties of new materials, predict the performance characteristics of products made of new materials, and increase the reliability of product hardness control.

About the Authors

A. E. Aslanyan
Russian Metrological Institute of Technical Physics and Radio Engineering
Russian Federation

Andrey E. Aslanyan

Mendeleevo, Moscow region



E. G. Aslanyan
Russian Metrological Institute of Technical Physics and Radio Engineering
Russian Federation

Edward G. Aslanyan

Mendeleevo, Moscow region



D. N. Pilipenko
Russian Metrological Institute of Technical Physics and Radio Engineering
Russian Federation

Demyan N. Pilipenko

Mendeleevo, Moscow region



V. V. Shvydun
Russian Metrological Institute of Technical Physics and Radio Engineering
Russian Federation

Vladimir V. Shvydun

Mendeleevo, Moscow region



A. N. Shchipunov
Russian Metrological Institute of Technical Physics and Radio Engineering
Russian Federation

Andrey N. Shchipunov

Mendeleevo, Moscow region



L. V. Yurov
Russian Metrological Institute of Technical Physics and Radio Engineering
Russian Federation

Lev V. Yurov

Mendeleevo, Moscow region



References

1. Doynikov A. S. (eds). Lectures on metrology. FSUE “VNIIFTRI”, Mendeleevo (2018). (In Russ.)

2. Aslanyan E. G., Pivovarov V. A., Aslanyan A. E. et al. National primary special standard for the Vickers metal hardness scale. Measurement Techniques, 55(5), 489–496 (2012). https://doi.org/10.1007/s11018-012-9987-x

3. Aslanyan E., Herrman K. Final report on COOMET Vickers PTB/VNIIFTRI key comparison (COOMET.M.H-K1.b and COOMET.M.H-K1.c), Metrologia, 50(1A), 070082013 (2013). https://doi.org/10.1088/0026-1394/50/1A/07008

4. Aslanyan A. E. Regional comparisons of National primary standards of hardness according to the Vickers and Brinell scales. Measurement Techniques. 64(8), 628–632 (2021). https://doi.org/10.1007/s11018-021-01982-6

5. Chicot D., Mercier D., Roudet F., Silva K., Staia M. H., Lesage J. Comparison of instrumented Knoop and Vickers hardness measurements on various soft materials and hard ceramics. Journal of the European Ceramic Society, 27(4), 1905– 1911 (2007). https://doi.org/10.1016/j.jeurceramsoc.2006.06.011

6. Yamamoto T., Yamamoto M., Hattori K. Study on methods for measuring Vickers indentations. HARDMEKO 2010 IMEKO 2010 TC3, TC5 and TC22 Conferences Metrology in Modern Context, Pattaya, Thailand, 22–25 November 2010.

7. Herrmann K. Knoop ISO 4545 and ASTM E284 Procedures. In K. Herrmann (eds). Hardness Testing Principles and Applications, pp. 62–65. ASM International, Novelty, USA (2011).

8. Giannakopoulos A. E., Zisis Th. Analysis of Knoop indentation. International Journal of Solids and Structures, 48(1), 175–190 (2011). https://doi.org/10.1016/j.ijsolstr.2010.09.014

9. Aslanyan E., Pivovarov V., Aslanyan A. et al. Load range expansion of national primary hardness standard machine on Vickers scales. XX IMEKO World Congress Metrology for Green Growth, Busan, Republic of Korea, 9–14 September, 2012.

10. Fabijanic T. A., Katic M., Alar Z., Menelao F. Comparison of Vickers hardness measurement in high hardness range. XXI IMEKO World Congress “Measurement in Research and Industry”, Prague, Czech Republic, August 30 – September 4, 2015. https://www.researchgate.net/publication/281460600

11. Prato A., Origlia C., Germak A. Verifi cation of Knoop indenters with a Vickers-addressed optical system. Measurement, 163, 107928 (2020). https://doi.org/ 10.1016/j.measurement.2020.107928

12. Sorokina P. V. Metrological investigation of a standard system for reproducing knoop hardness numbers. Al”manac of modern metrology, (2(30)), 89–93 (2022). (In Russ.) https://elibrary.ru/nggldz

13. Takagi S., Tanaka Y., Seino Y. Comparison of microscopic observation techniques to determine Vickers indentation diagonal length. IMEKO 14th TC5 Conference on the Measurement of Hardness (together with the 24th TC3 Conference on the Measurement of Force, Mass and Torque, the 6th TC16 Conference on Pressure and Vacuum Measurement, and the 5th TC22 Conference on Vibration Measurement), Cavtat-Dubrovnik, Croatia, 11–13 October 2022. https://doi.org/10.21014/tc5-2022.049


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For citations:


Aslanyan A.E., Aslanyan E.G., Pilipenko D.N., Shvydun V.V., Shchipunov A.N., Yurov L.V. State primary standard machine on Vickers and Knoop hardness scales GET 31-2024. Izmeritel`naya Tekhnika. 2024;73(12):7-13. (In Russ.) https://doi.org/10.32446/0368-1025it.2024-12-7-13

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ISSN 0368-1025 (Print)
ISSN 2949-5237 (Online)